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1 article(s) from Cézard, Christine

Synthesis and characterization of a new photoinduced switchable β-cyclodextrin dimer

Florian Hamon,
Claire Blaszkiewicz,
Marie Buchotte,
Estelle Banaszak-Léonard,
Hervé Bricout,
Sébastien Tilloy,
Eric Monflier,
Christine Cézard,
Laurent Bouteiller,
Christophe Len and
Florence Djedaini-Pilard

Beilstein J. Org. Chem. 2014, 10, 2874–2885, doi:10.3762/bjoc.10.304

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Graphical Abstract

Scheme 1: Synthesis pathway of the dimer AZO-CDim 1.

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Figure 1: Overlaid UV spectra of the irradiation of AZO-CDim 1 (a) from 0 to 120 min at 365 nm and then (b) f...

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Figure 2: HPLC quantification of the cis/trans ratio of AZO-CDim 1 before irradiation (left) and after irradi...

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Figure 3: Percentage of cis isomer of AZO-CDim 1 produced during photoisomerization cycles (c = 10⁻⁴ M, water...

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Figure 4: Representation of the most stable structures obtained for the azobenzene linker (a) for the trans c...

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Figure 5: Structure of the ditopic guest ADAdim 4.

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Figure 6: Titration of (a) β-CD (c = 0.8 mM) and (b) β-CD-NH₂ (c = 0.8 mM) by ADAdim 4 (c = 4 mM). (c) Diluti...

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Figure 7: (a) ¹H NMR spectra of AZO-CDim 1 (500 MHz, D₂O, 2.5 mM) in the absence (bottom) and presence of ADA...

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Figure 8: Proposed structures of inclusion complexes with the ditopic host AZO-CDim 1 and the ditopic guest A...

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Published 04 Dec 2014

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